Gas chromatography-isotope dilution mass spectrometry method validation for target pesticides in soybeans

References

• Alder L, Greulich K, Kempe G, Vieth B. 2006. Residue analysis of 500 high priority pesticides: better by GC-MS or LC-MS/MS? Mass Spectrom Rev. 25(6):838–865.
   PubMed Web of Science ®Google Scholar
• Cunha SC, Fernandes JO. 2011. Multipesticide residue analysis in maize combining acetonitrile-based extraction with dispersive liquid–liquid microextraction followed by gas chromatography–mass spectrometry. J Chromatogr. 1218(43):7748–7757.
   PubMed Web of Science ®Google Scholar
• David F, Devos C, Dumont E, Yang Z, Sandra P, Huertas-Pérez JF. 2017. Determination of pesticides in fatty matrices using gel permeation clean-up followed by GC-MS/MS and LC-MS/MS analysis: A comparison of low- and high-pressure gel permeation columns. Talanta. 165:201–210.
   PubMed Web of Science ®Google Scholar
• Domingos Alves R, Romero-González R, López-Ruiz R, Jiménez-Medina ML, Garrido Frenich A. 2016. Fast determination of four polar contaminants in soy nutraceutical products by liquid chromatography coupled to tandem mass spectrometry. Anal Bioanal Chem. 408(28):8089–8098.
   PubMed Web of Science ®Google Scholar
• Erney DR, Pawlowski TM, Poole CF. 1997. Matrix-induced peak enhancement of pesticides in gas chromatography: is there a solution? HRC J High Resolut Chromatogr. 20(7):375–378.
   Google Scholar
• EURACHEM Guide: The Fitness for Purpose of Analytical Methods. A Laboratory Guide to Method Validation and Related Topics. 2014. Magnusson B and Örnemark U, editor. 2nd ed.
   Google Scholar
• EURACHEM/CITAC Guide: Quantifying Uncertainty in Analytical Measurement. 2012. Ellison SLR and Williams A, editor. 3rd ed.
   Google Scholar
• European Commission 2002/657/EC 2002. Commission decision of 12 august 2002 implementing council directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. Official Journal of the European Communities. p. 29
   Google Scholar
• [FAO] Food and Agriculture Organization of the United Nations. 2017. FAOSTAT [Acccessed 2018 Jun] http://www.fao.org/faostat/en/#data/TP.
   Google Scholar
• García-Reyes JF, Ferrer C, Gómez-Ramos MJ, Fernández-Alba AR, García-Reyes JF, Molina-Díaz A. 2007. Determination of pesticide residues in olive oil and olives. TrAC Trends Anal Chem. 26(3):239–251.
   Web of Science ®Google Scholar
• Garrido Frenich A, Martínez Vidal JL, Cruz Sicilia AD, González Rodríguez MJ, Plaza Bolaños P. 2006. Multiresidue analysis of organochlorine and organophosphorus pesticides in muscle of chicken, pork and lamb by gas chromatography–triple quadrupole mass spectrometry. Anal Chim Acta. 558(1):42–52.
   Web of Science ®Google Scholar
• Garrido Frenich A, Martínez Vidal JL, Fernández Moreno JL, Romero-González R. 2009. Compensation for matrix effects in gas chromatography–tandem mass spectrometry using a single point standard addition. J Chromatogr. 1216(23):4798–4808.
   PubMed Web of Science ®Google Scholar
• Gilbert-López B, García-Reyes JF, Molina-Díaz A. 2009. Sample treatment and determination of pesticide residues in fatty vegetable matrices: a review. Talanta. 79(2):109–128.
   PubMed Web of Science ®Google Scholar
• Hajšlová J, Zrostlı́ková J. 2003. Matrix effects in (ultra)trace analysis of pesticide residues in food and biotic matrices. J Chromatogr. 1000(1):181–197.
   Web of Science ®Google Scholar
• Hirahara Y, Kimura M, Inoue T, Uchikawa S, Otani S, Haganuma A, Matsumoto N, Hirata A, Maruyama S, Iizuka T, et al. 2005. Validation of multiresidue screening methods for the determination of 186 pesticides in 11 agricultural products using gas chromatography (GC). J Health Sci. 51(5):617–627.
   Web of Science ®Google Scholar
• Huertas Pérez JF, Sejerøe-Olsen B, Fernández Alba AR, Schimmel H, Dabrio M. 2015. Accurate determination of selected pesticides in soya beans by liquid chromatography coupled to isotope dilution mass spectrometry. Talanta. 137:120–129.
   PubMed Web of Science ®Google Scholar
• International Organization for Standardization. 1994. ISO 5725-1:1994 - accuracy (trueness and precision) of measurement methods and results - Part 1: general principles and definitions. Geneva: ISO.
   Google Scholar
• International Organization for Standardization. 2010. ISO 21748:2010 - guidance for the use of repeatability, reproducibility and trueness estimates in measurement uncertainty estimation. Geneve: ISO.
   Google Scholar
• International Organization for Standardization. 2017a. ISO/IEC 17025:2017. General requirements for the competence of testing and calibration laboratories. Geneva: ISO.
   Google Scholar
• International Organization for Standardization. 2017b. ISO/IEC Guide 35 Reference materials – general and statistical principles for certification. Geneva: ISO.
   Google Scholar
• Kim K-G, Park D-W, Kang G-R, Kim T-S, Yang Y, Moon S-J, E-A C, D-R H, E-S K, B-S C. 2016. Simultaneous determination of plant growth regulator and pesticides in bean sprouts by liquid chromatography–tandem mass spectrometry. Food Chem. 208:239–244.
   PubMed Web of Science ®Google Scholar
• Kumar V, Rani A, Solanki S, Hussain SM. 2006. Influence of growing environment on the biochemical composition and physical characteristics of soybean seed. J Food Composition Anal. 19(2):188–195.
   Web of Science ®Google Scholar
• LeDoux M. 2011. Analytical methods applied to the determination of pesticide residues in foods of animal origin. A review of the past two decades. J Chromatogr. 1218(8):1021–1036.
   PubMed Web of Science ®Google Scholar
• Lehotay SJ, Mastovska K, Lightfield AR, Gates RA. 2010. Multi-analyst, multi-matrix performance of the QuEChERS approach for pesticide residues in foods and feeds using HPLC/MS/MS analysis with different calibration techniques. J AOAC Int. 93(2):355–367.
   PubMed Web of Science ®Google Scholar
• Li Z, Li Y, Liu X, Li X, Zhou L, Pan C. 2012. Multiresidue analysis of 58 pesticides in bean products by disposable pipet extraction (DPX) cleanup and gas chromatography-mass spectrometry determination. J Agric Food Chem. 60(19):4788–4798.
   PubMed Web of Science ®Google Scholar
• Linsinger TPJ, Pauwels J, Van Der Veen AMH, Schimmel H, Lamberty A. 2001. Homogeneity and stability of reference materials. Accreditation Qual Assur. 6(1):20–25.
   Web of Science ®Google Scholar
• Maldaner L, Santana CC, Jardim ICSF. 2008. HPLC determination of pesticides in soybeans using matrix solid phase dispersion. J Liquid Chromatogr Relat Technologies. 31(7):972–983.
   Web of Science ®Google Scholar
• May MM, Ferronato G, Bandeira NMG, Prestes OD, Zanella R, Adaime MB. 2017. Determination of pesticide residues in soy-based beverages using a QuEChERS method (with clean-up optimized by central composite design) and ultra-high-performance liquid chromatography-tandem mass spectrometry. Food Analytical Methods. 10(2):369–378.
   Web of Science ®Google Scholar
• Messina M. 1997. Soyfoods: their role in disease prevention and treatment. In: Liu K, editor. Soybean chemistry and utilisation. New York: Chapman and Hall; p. 442–477.
   Google Scholar
• Nguyen TD, Lee MH, Lee GH. 2010. Rapid determination of 95 pesticides in soybean oil using liquid–liquid extraction followed by centrifugation, freezing and dispersive solid phase extraction as cleanup steps and gas chromatography with mass spectrometric detection. Microchemical J. 95(1):113–119.
   Web of Science ®Google Scholar
• Páleníková A, Martínez-Domínguez G, Arrebola FJ, Romero-González R, Hrouzková S, Frenich AG. 2015. Multifamily determination of pesticide residues in soya-based nutraceutical products by GC/MS–MS. Food Chem. 173:796–807.
   PubMed Web of Science ®Google Scholar
• Pizzutti IR, de Kok A, Hiemstra M, Wickert C, Prestes OD. 2009. Method validation and comparison of acetonitrile and acetone extraction for the analysis of 169 pesticides in soya grain by liquid chromatography-tandem mass spectrometry [Article]. J Chromatogr. 1216(21):4539–4552.
   PubMed Web of Science ®Google Scholar
• Pizzutti IR, de Kok A, Zanella R, Adaime MB, Hiemstra M, Wickert C, Prestes OD. 2007. Method validation for the analysis of 169 pesticides in soya grain, without clean up, by liquid chromatography–tandem mass spectrometry using positive and negative electrospray ionization. J Chromatogr. 1142(2):123–136.
   PubMed Web of Science ®Google Scholar
• Presta MA, Kolberg DIS, Wickert C, Pizzutti IR, Adaime MB, Zanella R. 2009. High resolution gel permeation chromatography followed by GC-ECD for the determination of pesticide residues in soybeans. Chromatographia. 69(3–4):237–241.
   Web of Science ®Google Scholar
• Raina-Fulton R. 2015. New trends in pesticide residue analysis in cereals, nutraceuticals, baby foods, and related processed consumer products. J AOAC Int. 98(5):1163–1170.
   PubMed Web of Science ®Google Scholar
• European Commission. 2005. Regulation EC/396/2005 of the European Parliament and of the Council of February 23. on maximum residue levels of pesticides in or on food and feed of plant and animal origin and amending council directive 91/414/EEC. Strasbourg: Official Journal of the European Union. p. 16.
   Google Scholar
• European Commission. 2017. SANTE/11813/2017. Guidance document on analytical quality control and method validation procedures for pesticides residues analysis in food and feed. European Commission Directorate-General for Health and Food Safety; [Accessed Jan 2018].https://ec.europa.eu/food/sites/food/files/plant/docs/pesticides_mrl_guidelines_wrkdoc_2017-11813.pdf
   Google Scholar
• Sejeroe-Olsen B, Shegunova P, Grimalt Brea S, Harbeck S, Fernandez-Alba A.R.Dabrio M. 2014. Certified reference material for pesticide residue analysis: how to deal with thousands of pesticide-matrix combinations? 10th European pesticide residue workshop. https://www.eprw2014.com
   Google Scholar
• Van Der Veen AMH, Linsinger T, Pauwels J. 2001. Uncertainty calculations in the certification of reference materials. 2. Homogeneity study. Accreditation Qual Assur. 6(1):26–30.
   Web of Science ®Google Scholar
• Viera MS, Rizzetti TM, de Souza MP, Martins ML, Prestes OD, Adaime MB, Zanella R. 2017. Multiresidue determination of pesticides in crop plants by the quick, easy, cheap, effective, rugged, and safe method and ultra-high-performance liquid chromatography tandem mass spectrometry using a calibration based on a single level standard addition in the sample. J Chromatogr. 1526:119–127.
   Web of Science ®Google Scholar
• Villaverde JJ, Sevilla-Morán B, López-Goti C, Alonso-Prados JL, Sandín-España P. 2016. Trends in analysis of pesticide residues to fulfil the European regulation (EC) No. 1107/2009. TrAC Trends Anal Chem. 80:568–580.
   Web of Science ®Google Scholar
• Wang J, Cheung W, Chow W. 2013. Ultra-high performance liquid chromatography/electrospray ionization-tandem mass spectrometry determination of 151 pesticides in soybeans and pulses. J AOAC Int. 96(5):1114–1133.
   PubMed Web of Science ®Google Scholar
• Wu G, Bao X, Zhao S, Wu J, Han A, Ye Q. 2011. Analysis of multi-pesticide residues in the foods of animal origin by GC–MS coupled with accelerated solvent extraction and gel permeation chromatography cleanup. Food Chem. 126(2):646–654.
   Web of Science ®Google Scholar
• Xinyi C, Xiwu G, Xiaogang C, Wei Y, Yun L, Mingli Y, Xiuqing L, Daning W, Yanyan F, Zweigenbaum JA. 2007. Application of liquid chromatography-time-of-flight-mass spectrometry for the analysis of urea herbicides residues in soybean. Anal Lett. 40(6):1117–1130.
   Web of Science ®Google Scholar
• Yarita T, Otake T, Aoyagi Y, Kuroda Y, Numata M, Iwata H, Watai M, Mitsuda H, Fujikawa T, Ota H. 2014. Development of soybean certified reference material for pesticide residue analysis. Talanta. 119:255–261.
   PubMed Web of Science ®Google Scholar