High throughput residue analysis of paraquat and diquat involving hydrophilic interaction liquid chromatographic separation and mass spectrometric determination

References

• Anastassiades M, Kolberg DI, Benkenstein A, Eichhorn E, Zechmann S, Mack D, Wildgrube C, Sigalov I, Dork D, Barth A. October 2016. QuPPe-method, version 9.2; [accessed 2017 Nov 30]. http://www.eurl-pesticides.eu/userfiles/file/EurlSRM/meth_QuPPe-PO_EurlSRM.pdf
   Google Scholar
• Annesley TM. 2003. Ion suppression in mass spectrometry. Clin Chem. 49:1041–1044.
   PubMed Web of Science ®Google Scholar
• Banerjee K, Oulkar DP, Dasgupta S, Patil SB, Patil SH, Savant R, Adsule PG. 2007. Validation and uncertainty analysis of a multi-residue method for pesticides in grapes using ethyl acetate extraction and liquid chromatography–tandem mass spectrometry. J Chromatogr A. 1173:98–109.
   PubMed Web of Science ®Google Scholar
• Buszewski B, Noga S. 2012. Hydrophilic interaction liquid chromatography (HILIC)—a powerful separation technique. Anal Bioanal Chem. 402:231–247.
   PubMed Web of Science ®Google Scholar
• Chamkasem N, Morris C, Harmon T. 2017. Determination of paraquat and diquat in potato by liquid chromatography/tandem mass spectrometer. J Reg Sci. 5:1–8.
   Google Scholar
• CIBRC. Registered under section 9 (3) of the insecticides Act, 1968 for use in the Country: as on 30/06/2017; [accessed 2017 Dec 10]. http://www.cibrc.nic.in/Insecticides/Pesticides
   Google Scholar
• Esparza X, Moyano E, Galceran M. 2009. Analysis of chlormequat and mepiquat by hydrophilic interaction chromatography coupled to tandem mass spectrometry in food samples. J Chromatogr A. 1216:4402–4406.
   PubMed Web of Science ®Google Scholar
• EU Pesticide Database. [accessed 2017 Dec 01]. http://ec.europa.eu/food/plant/pesticides/eu-pesticides-database/public/?event=pesticide.residue.CurrentMRL&language=EN
   Google Scholar
• Florêncio MH, Pires E, Castro AL, Nunes MR, Borges C, Costa FM. 2004. Photodegradation of diquat and paraquat in aqueous solutions by titanium dioxide: evolution of degradation reactions and characterisation of intermediates. Chemosphere. 55:345–355.
   PubMed Web of Science ®Google Scholar
• Grey L, Nguyen B, Yang P. 2002. Liquid chromatography–electrospray ionization isotope dilution mass spectrometry analysis of paraquat and diquat using conventional and multilayer solid-phase extraction cartridges. J Chromatogr A. 958:25–33.
   PubMed Web of Science ®Google Scholar
• Guijarro EC, Yanez-Sedeno P, Diez LP. 1987. Determination of paraquat by flow-injection spectrophotometry. Anal Chim Acta. 199:203–208.
   Web of Science ®Google Scholar
• Hao C, Zhao X, Morse D, Yang P, Taguchi V, Morra F. 2013. Optimized liquid chromatography tandem mass spectrometry approach for the determination of diquat and paraquat herbicides. J Chromatogr A. 1304:169–176.
   PubMed Web of Science ®Google Scholar
• Kolberg DI, Mack D, Anastassiades M, Hetmanski MT, Fussell RJ, Meijer T, Mol HG. 2012. Development and independent laboratory validation of a simple method for the determination of paraquat and diquat in potato, cereals and pulses. Anal Bioanal Chem. 404:2465–2474.
   PubMed Web of Science ®Google Scholar
• Koley TK, Khan Z, Oulkar D, Singh B, Maurya A, Singh B, Banerjee K. 2017. High resolution LC-MS characterization of phenolic compounds and the evaluation of antioxidant properties of a tropical purple radish genotype. Arabian J Chem. doi:10.1016/j.arabjc.2017.11.007
   Google Scholar
• Mallet CR, Lu Z, Mazzeo JR. 2004. A study of ion suppression effects in electrospray ionization from mobile phase additives and solid‐phase extracts. Rapid Commun Mass Spectrom. 18:49–58.
   PubMed Web of Science ®Google Scholar
• The Pesticide Manual. 2012. British crop protection council. 16th ed. Alton (UK): British crop protection council.
   Google Scholar
• Pizzutti IR, Vela GM, de Kok A, Scholten JM, Dias JV, Cardoso CD, Concenço G, Vivian R. 2016. Determination of paraquat and diquat: LC-MS method optimization and validation. Food Chem. 209:248–255.
   PubMed Web of Science ®Google Scholar
• SANTE/11813/2017. [accessed 2018 Jan 10]. https://ec.europa.eu/food/sites/food/files/plant/docs/pesticides_mrl_guidelines_wrkdoc_2017-11813.pdf
   Google Scholar
• Takino M, Daishima S, Yamaguchi K. 2000. Determination of diquat and paraquat in water by liquid chromatography/electrospray-mass spectrometry using volatile ion-pairing reagents. Ana Sci. 16:707–711.
   Web of Science ®Google Scholar
• Tsao Y-C, Lai Y-C, Liu H-C, Liu RH, Lin D-L. 2016. Simultaneous determination and quantitation of paraquat, diquat, glufosinate and glyphosate in postmortem blood and urine by LC-MS-MS. J Anal Toxicol. 40:427–436.
   PubMed Web of Science ®Google Scholar
• Ugare B, Banerjee K, Ramteke S, Pradhan S, Oulkar DP, Utture SC, Adsule PG. 2013. Dissipation kinetics of forchlorfenuron, 6-benzyl aminopurine, gibberellic acid and ethephon residues in table grapes (Vitis vinifera). Food Chem. 141:4208–4214.
   PubMed Web of Science ®Google Scholar
• Van Nuijs AL, Tarcomnicu I, Covaci A. 2011. Application of hydrophilic interaction chromatography for the analysis of polar contaminants in food and environmental samples. J Chromatogr A. 1218:5964–5974.
   PubMed Web of Science ®Google Scholar
• Wang K-C, Chen S-M, Hsu J-F, Cheng S-G, Lee C-K. 2008. Simultaneous detection and quantitation of highly water-soluble herbicides in serum using ion-pair liquid chromatography–tandem mass spectrometry. J Chromatogr B. 87:211–218.
   Google Scholar
• Wang Z, Wang Z, Xing J. 2011. The quantitative analysis of paraquat in biological samples by liquid chromatography-electrospray ionization-mass spectrometry. J Anal Toxicol. 35:23–27.
   PubMed Web of Science ®Google Scholar
• Whitehead RD Jr., Montesano MA, Jayatilaka NK, Buckley B, Winnik B, Needham LL, Barr DB. 2010. Method for measurement of the quaternary amine compounds paraquat and diquat in human urine using high-performance liquid chromatography–tandem mass spectrometry. J Chromatogr B. 878:2548–2553.
   PubMed Web of Science ®Google Scholar
• Zou T, He P, Cao J, Li Z. 2014. Determination of paraquat in vegetables using HPLC–MS-MS. J Chromatogr Sci. 53:204–209.
   PubMed Web of Science ®Google Scholar